• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    SUMMARY A process for batch leaching of fire lime in a slacker (2), in which a lime sludge is produced with a high degree of fineness and long sedimentation time, comprising the following process steps: control of the leaching temperature is carried out in two phases - in a first phase at incoming water temperatures between 0 -10 ° C a predetermined amount of the finished sludge is discharged - in a second phase at incoming water temperatures between 10-20 ° C a predetermined amount of rinsing water or sod water is added.
    公开号:SE537518C2
    申请号:SE1251348
    申请日:2011-04-28
    公开日:2015-06-02
    发明作者:Poju R Stephansen
    申请人:Poju R Stephansen As；
    IPC主号:
    专利说明:

    The present invention relates to a process for temperature control for batch quenching of fire lime in a slacker, in which a lime sludge is produced, as stated in the introduction to the independent claim. and long sedimentation time.
    Lime varnishes of various types, most of which are intended for continuous operation, have been used industrially for some time. "W + T" and "BJF" slackers can be referred to as examples.
    U.S. Pat. No. 4,547,349 relates to a device for non-batch, continuous leaching of lime. UK patent application GB 2048107A discloses and describes a lime varnish, also for non-batch continuous operation. EPpatentansokan 0510675A3 refers to a lime varnish for non-batch continuous operation. CA patent application 1212825 relates to a regulated process for batch production of slaked lime.
    Furthermore, US 7,105,146 B2 discloses a method for batch leaching of lime which includes a rinsing step before the subsequent leaching.
    Continuous lime painters have in common that they are responsive to control, very maintenance-intensive, not suitable for computer-controlled operation and expensive to manufacture.
    The NO patent application 19933084, previously filed by the present applicant PR Stephansen, describes a method for batch slackening, so-called "batch slackening" of burnt lime, even in relatively small amounts in relation to the slacker's volume, after which a finished product with relatively low lime concentration is obtained. .
    The content of the present application is a further development of NO 319297 and NO 327528, previously filed patent applications NO 19980435 and NO 20070890 by the present applicant P R Stephansen, and which are hereby incorporated by reference. 1 During operation of a lime slacker, contaminants and dust can cause limestone to accumulate, which affects slackening and can cause blowouts at high temperatures. It is an object of the present invention to provide a new method for controlling the temperature, especially in connection with variable water temperatures into the slacker, which prevents the accumulation of limestone and the disadvantages this leads to.
    A closed system is created that does not produce dust, and depending on the immediate cleaning and temperature control, an installation is provided with, at least, significantly reduced maintenance due to the reduction of the accumulation of limestone.
    Through the characterizing part of claim 1, the present invention is characterized in that the control of the quenching temperature is carried out in one of at least two phases depending on the temperature of the inlet water, in which: in a first phase at water temperatures between 0-10 ° C, the temperature is controlled in a predetermined amount more of the finished sludge is discharged if a lower temperature limit has not been reached, and if the temperature during slacking exceeds an upper temperature limit until a predetermined amount less of the finished sludge is released, and in a second phase at water temperatures between 10-20 ° C, the temperature is regulated in that more of a predetermined amount of rinsing water or spawning water is added if a lower temperature limit is not reached, and if the temperature during slacking exceeds an upper temperature limit is added less of a predetermined amount of rinsing water or spading water.
    Alternative preferred embodiments of the invention are characterized by the dependent claims 2-5.
    The second phase with more or less supply of rinsing water or sod water is preferably activated when the first phase has regulated the emptying level up to a predetermined number of times.
    The amount of more or less finished sludge that is emptied and the amount of more or less rinsing water or sod water that can be added can be regulated depending on the capacity of the slacker. 2 In a slacker with a capacity of 4,000 kg, at a water temperature between 0-10 ° C, the temperature can be regulated in the first phase in that 50 kg more of the finished sludge is discharged if a lower temperature limit of 79 ° C is not and if the temperature during slacking exceeds an upper temperature limit of 86 ° C, 50 kg less of the finished sludge can be emptied out.
    In a slacker with a capacity of 4,000 kg and water temperatures between 10-20 ° C, the temperature can be regulated in the second phase in that 50 kg more of the rinsing water or sod water is added if a lower temperature limit of 79 ° C is not reached, and if the temperature during slacking If the upper temperature limit exceeds 86 ° C, 50 kg less rinsing water or sod water can be added.
    The invention will be described with the aid of the accompanying figure which shows an exemplary embodiment of a lime varnish device.
    By carrying out the method according to the invention for batch hot leaching of fire lime, a lime leaching device is used as shown and described in detail in the said NO patent application 19933084, to which reference is made.
    It should be noted that the values for given weights, volumes, temperatures, times, etc. are given as examples, and the said values must therefore not be regarded as absolute.
    An example of a lime leaching device, which is shown schematically in Figure 1, essentially comprises a lime lacquer 2 with a cylindrical upper part 53 and a conical lower part 54 mounted on three load cells 7 for batchwise weighing of water and lime and with a mixer 16 with a specially designed mixing body and drive motor 18, rotation monitor 20 and also a water jet driven combined vacuuming / evaporation device / intermediate wall 15 which is supplied with water through a pipeline with a valve 17, where the slacker 2 receives water through a pipeline with valves 8 and 9. The slack lid 4 is connected to a specially designed water outlet prevention valve which also separates the wet and dry lime zones. The slacker is connected to a lime silo 1 with a level indicator and also a filter 52 with a drive motor 51 for mechanical cleaning. The silo can hold 80 t of fire lime, for example with a bulk density of 1.1 (weight scale range 0-90 t), and is equipped with load cells to unload the weight. The amplifiers of the load cells 3 emit a 4-20 mA signal to a PLC. SiIon can also be equipped with three air activators that start and follow a given cycle if the dosing time for the screw conveyor is exceeded.
    SiIon is filled with lime through the inlet pipe from, for example, a tanker.
    The weight of the amount in the silo shows Iran a cabinet at the silo filling site. When 95 `) / 0 of the weight (AH) has been reached, an alarm is given in the form of an audible / light signal such as a warning that the filling must be stopped. The audible alarm can be set up and / or automatically by means of the PLC, for example after three minutes. At 100 wt / l (AHH), a fill valve closes automatically and the charge of lime is stopped. While the valve is closed, a red warning light in the cabinet indicates that the silo cannot be refilled. The filling valve can be controlled manually from the panel in the control center.
    Load cells mounted on the silo send out an alarm signal and a trip signal: at AHLarm. The operator is asked about a hog niya in the silo. at AHHVarnar the operator and closes the inlet valve. - at ALZLarm. Lag niva i silon.
    The filter motor is preferably equipped with a safety switch and an operating switch (automatic / manual).
    After the filling of lime in the silo has been completed, the filter motor 51 is started manually in a local cabinet. A signal is sent from the cabinet to an external PLC which starts the filter motor and monitors the operating condition of the motor. The filter motor 51 stops automatically after three minutes.
    Example Start button in a local cabinet is activated The filter motor 51 starts and the operating light in the cabinet turns on. The filter motor stops after about three minutes. Lime is transferred with the screw conveyor 6 from silo 1 to the slacker 2 with the valves 11 and 12 open. The slackening is initiated in that the first batch is slackened manually. The addition of lime then takes place automatically, whereby the slacker 2 is filled with a predetermined amount of sod water. The slacker is then emptied 4 to a predetermined remaining amount, in which the next batch of lime is to be quenched.
    The lime leaching temperature is determined by the ratio between the remaining number of kilos of diluted lime sludge in the slacker (EVL) and the number of kilos of added lime (EVH), or the selected installation points on the load cells 7, ie the installation points on the scale selected. The concentration of slaked lime is finally determined by the number of kilograms of water selected at the last installation point (EVHH). The number of kilograms of water obtained at the last installation point (EVHH) is decisive for the concentration of completely slaked lime.
    The load cells 7 generate four operating contacts for use in sequence: at EVHHHFilling of water to the upper level. - in case of EVHHUnded amount of filled flush water. at EVHUpent amount of added lime. at EVLNy slackening level confirmed for fly slackening. at EVLLO stirring is stopped.
    Whole slaked lime is conveyed to a storage tank 3 through the valve 22 by means of an engine. The motor is preferably equipped with a safety switch and an operating switch.
    The following first example shows a slacker with a working volume of, for example, 2,1001 (weight range 0-2,500 kg). At the start, the slacker is filled 2 times with 400 l of water, followed by 120 kg of lime while stirring. When the mixture has reached a stable temperature of about 80 ° C, registered by a temperature supply element, automatic operation can start and water is added to a mixing weight of 1,200 kg, giving a 10 "Yo sludge with a temperature of about 30 ° C.
    The slacker can now be emptied to a residual weight of, for example, 600 kg. This is followed by an interruption of 30 s before returning from, for example, the pump. It is important that the control system can register the actual value of the batch and is tarred to 0 kg, which is necessary as fidelity in the system can lead to a risk that more or more chemicals than predetermined additives are added to the slacker.
    With automatic control, when the weight of the slacker 2 is 600 kg or a new calculated value based on the temperature control and after a pause of 30 s, the slackening process will start if it is not already running and the valve 22 will close.
    The valve 12 in the slacker lid receives an opening signal and is confirmed in an open position. After 5 s time delay, the valve 11 is opened at the discharge sand by the screw conveyor 6 and, as in the case of Oppen Than, a check switch is confirmed. A rotation monitor checks that the stirring has started and an alarm is issued if this is not the case or if the valve is not open after the command. If the stirring stops, the valve 9 is opened and the slacker is completely filled with water and the process is stopped.
    The screw conveyor 6 is started 5 s after a check switch has confirmed that the valve 11 is in an open position, and starts the timer for normal dosing time, for example 180 s. The correct dosing time is set when initiating the system. If the time is exceeded by 100% (360 in this example), the air stimulator will be opened and barred in a fixed cycle (open for about 0.5 s every 30 s) with the beginning of the break and limited to 180 s. If the predetermined weight in the mixer is still not opened, the cycle will be interrupted because the storage tank signals a low level and an alarm is issued.
    The screw conveyor 6 is kept running until the required amount of lime (120 kg) has been weighed in. 1 s after the conveyor has stopped, the valve 11 is closed. 10 s after the valve is confirmed as closed, a solenoid valve is opened for 3 s for air to the effluent vibrator. The valve 12 is closed for 20 s after the valve 11 is confirmed to be closed, and a check switch checks that the valve is closed. When the valve has been closed, the weight is recalibrated to 0 kg. An alarm sounds if the valve is not closed after the command.
    For immediate cleaning of the slacker 2 before slackening, after said tareing of the load cell installation 7, a number of valves can be opened during a fixed period of time for supplying rinsing water to the respective nozzles, in that the rinsing water is supplied sequentially via the usual nozzle (s) until a predetermined amount of rinsing water is obtained in the slacker 2. For example, 5 s after the valve in the slacker 2 has signaled closed and after the finished slackening, the first valve 25 for rinsing water with 6 a nozzle for 10 s is opened, after which the first valve 25 and the second valve 26 is opened for rinsing water with three nozzles for 8 s, after which the second valve 26 is closed and the third valve 27 is opened for rinsing water with three nozzles on the opposite side of the slacker 2, until a total predetermined amount of rinsing water has been weighed in. in the slacker. Rinsing water is supplied until the total amount of rinsing water weighed in is, for example, 20 kg.
    As shown in the figure, the first valve 25 controls the supply of water to one or more nozzles via a pipe 28, while the second valve controls the supply of water to one or more nozzles via a pipe 29 and the third valve 27 controls the supply of water to a or several nozzles via a pipeline 30. Preferably, nozzles are located on opposite sides of the slacker, for example the nozzles may be located in one half of the circumference or the whole circumference of the slacker, for example at the same or different inboard spaces. 20s after the valve 12 is closed, the shut-off signal is delivered to the valve 17 and the vacuuming 15 is stopped. After the screw conveyor is stopped, the adjustable slackening time is drilled, for example 10 min. The selected slack time and the course thereof must be indicated to the operator.
    When the slacking time is over, water is supplied through the valve 8 and through the flushing nozzles 24 for 15 s. / 0 lime sludge at a temperature of 30 ° C. With an error of added amount of lime that is Over +2 (:) / 0, the amount of sod water is adjusted.
    The temperature in the slacker is monitored by a temperature supply element. If a temperature of 83 ° C is not reached during the slackening process, an additional 15 kg of the finished sludge is discharged, thereby reducing EVLL to 485 kg or conversely the temperature is too high (88 ° C) to 515 kg.
    If the temperature during the slackening process rises Above 96 ° C, also open valve 8, or other valves, the slacker is filled with water to full level EVHHH, the process is interrupted and an alarm is given, without stopping the stirring.
    As previously described, for the production of a 10% lime sludge, 60 kg of lime and 600 kg of water are added. The total level will vary 7 depending on the temperature control. The final concentration of the lime sludge is decisive for the temperature of the slain to which the lime was added for the next slackening. If a lime sludge with a higher concentration is desired, slackening should take place at a higher initial temperature. If a lower concentration is required, for example at the use shed, the sludge should be shoveled out outside the slacker, for example by proportional dosing between water and limescale in the pipeline after the storage tank. Addition of water can be regulated with a river feeder and a control valve. Alternatively, metered amounts of water can be added to the storage tank at the same time as the slacker, from full weight in smaller batches, for example four, adds proportional amounts of lime sludge to the storage tank.
    After the slackening time has elapsed, the level in the storage tank is checked and when this is reduced to EVLL, the valve 22 is opened and the batch is emptied into the storage tank.
    In a second example, a slacker with a capacity of, for example, 4,000 kg is used. It will be described in connection with such a slacker how the temperature control can be performed in several phases depending on the inlet water temperature. The final amounts of more or less of the finished sludge discharged from the slacker and the amount of more or less of the rinsing water or sod water added to the slacker will thus be regulated depending on the capacity of the slacker.
    At water temperatures between 0-10 ° C, the temperature can be regulated in that a predetermined amount more of the finished sludge is discharged if a lower temperature limit is not reached, and if the temperature during slacking exceeds an upper temperature limit, a predetermined smaller amount of the finished sludge is discharged . In a slacker 2 with a capacity of 4,000 kg, 50 kg more of the finished sludge can be emptied if a lower temperature limit of 79 ° C is not reached, and if the temperature during slacking exceeds an upper temperature limit of 86 ° C, 50 kg less of it the finished sludge is emptied out.
    At water temperatures between 10-20 ° C, the temperature is regulated in that more of a predetermined amount of rinsing water or sod water is supplied if the lower temperature limit is not reached, and if the temperature during slacking exceeds an upper temperature limit, less of a predetermined amount of rinsing water or sod water is supplied. Correspondingly, in a slacker 2 with a capacity of 4,000 kg, the temperature in the second phase is regulated in that 50 kg more of 8 rinsing water or sod water is supplied if the lower temperature limit of 79 ° C is not reached, and if the temperature during slacking exceeds an upper temperature limit of 86 ° C added 50 kg less rinsing water or sod water.
    The second phase with more or less added rinsing water or sod water is activated, for example, when the first phase has regulated the emptying level up a predetermined number of times, such as EVL four times up.
    Similarly, as explained in the first example, if the temperature in phase one or phase two sometimes exceeds 96 ° C during the process, the valves are opened and the slacker is filled with water to (EVHHH) the full level and the process is stopped with the following equipment alarm. The mixer must not be stopped.
    Finished lime sludge is temporarily stored in the storage tanks 3 which are equipped with a level knob in the form of a pressure sensor and also one or more mixers. The tank can generate signals for regulating the slackening sequence. The level signal generates two operating contacts for use in the sequence and also two signals for alarms at low and high levels, respectively, and a signal for starting pumps. - at EVL: at EVLL: at AHH: at AL: at ALL: Slacking can be initiated.
    Signal for receiving a new batch of slacker. Alarm, niva alltfOr hog. Valve rod.
    Alarm, level too low.
    Alarm, very low level. Pumping out of storage tank 3 is stopped.
    The mixer must work continuously and be monitored by means of the PLC. One alarm is sounded in addition to the stop.
    One or more pumps are used for dosing the sludge. The pumps are arranged "standby" for each other and can be reset manually. Tacking water is added to the pumps' stuffing boxes through solenoid valves, which have built-in circuit breakers to release water if the tapping water does not appear for more than 3 minutes after start, an alarm is sounded and the pumps stop. The same will happen if tapping water is absent for three minutes during operation. In addition, each pump is equipped with a river detector and a pressure sensor mounted in the pipe on the pressure side of the pumps. If these do not register a large amount of water and pressure after 15 s, an alarm is issued. If the amount of water and 9 pressure is absent for another 15 s, the pumps will stop. A river feeder is used to feed the amount of sludge from the storage tank to the sand filter. This power supply transmits a 4-20 mA signal back to one or more frequency converters. Bottom set TOrns out of the storage tank through a nanoual shot bottom valve.
    In the two examples given above which describe slackers with a capacity of 2,100 kg and 4,000 kg, respectively, the normal slacking range is between 75 ° C and 90 ° C. Therefore, the given temperatures may not be considered as absolute, but are considered as examples, so that if slacker in the design examples and other slackers with different capacities, the temperatures may vary according to the circumstances.
    权利要求:
    Claims (5)
    [1]
    Automatic connection of a control system for automatic operation after the desired slackening temperature has been reached in the first batch, which adds soda water and then burns lime in a predetermined amount in the subsequent steps; 2. automatic control of the slackening temperature in the subsequent sludge batch, where the ratio between water and lime is adjusted if the desired slackening temperature was not reached or passed in the previous batch and where the slacker (2) is completely filled with water to stop the slacking if the maximum temperature is exceeded; and 3. automatic registration of the remaining amount of sludge in the slacker after completion of dosing of lime, and subsequent tarring of a load cell installation (7) to 0 kg before the next slackening, characterized in that the regulation of the slackening temperature is carried out in one of at least two phases, depending on temperature on the incoming water, in which 4. in a first phase at water temperatures between 0-10 ° C, the temperature is regulated in that a predetermined amount more of the finished sludge is emptied out if a lower temperature limit is not reached, and if the temperature during the slacking exceeds an upper temperature limit empties a predetermined amount less of the finished sludge, and 5. in a second phase at water temperatures between 10-20 ° C, the temperature is regulated in that more of a predetermined amount of rinsing water or sod water is added if a lower temperature limit is not reached , and if the temperature exceeds an upper temperature limit during slackening, less of a predetermined amount of rinsing water or sod water.
    [2]
    Method according to claim 1, characterized in that the second phase with more or less rinsing water or spade water added is activated when the first phase has regulated the emptying level up to a predetermined number of times. 11
    [3]
    Process according to Claim 1, characterized in that the amount of finished sludge which is emptied and the amount of rinsing water or sod water which is added are regulated depending on the capacity of the slacker.
    [4]
    Process according to claim 3, characterized in that the temperature is regulated in the first phase in a slacker (2) with a capacity of 4,000 kg and at water temperatures between 0-10 ° C in that 50 kg more of the finished sludge is discharged if a lower temperature limit of 79 ° C is not reached, and if the temperature during slacking exceeds the upper temperature limit of 86 ° C to less than 50 kg of the finished sludge out.
    [5]
    Method according to claim 3, characterized in that the temperature is regulated in the second phase in a slacker (2) with a capacity of 4,000 kg and at water temperatures between 10-20 ° C in that 50 kg more rinsing water or sod water is added if a lower temperature limit of 79 ° C is not reached, and if the temperature during slacking exceeds the Upper temperature limit of 86 ° C, 50 kg less of the rinsing water or sod water is added. 12 1/1
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    同族专利:
    公开号 | 公开日
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    EP2593410A1|2013-05-22|
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    NO327528B1|2007-02-16|2009-08-03|Poju R Stephansen As|Procedure for batch leaching of burnt lime into a liquor|
    NO328907B1|2007-06-25|2010-06-14|Poju R Stephansen As|Process for continuous and proportional lime addition to a water flow in a plant|CN105541136B|2016-01-20|2017-07-25|湖州浙宝冶金辅料有限公司|A kind of calcium hydroxide production technology and system|
    法律状态:
    优先权:
    申请号 | 申请日 | 专利标题
    NO20100611A|NO333228B1|2010-04-28|2010-04-28|Procedure for temperature control by batch-leaching of burnt lime in a liquor|
    PCT/NO2011/000139|WO2011136658A1|2010-04-28|2011-04-28|Method for temperature control in a slaker|
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